Kohlensäurebis(trimethylsilyl)ester: Spektroskopische Charakterisierung und verbesserte Darstellung/ The Bis(trimethylsilyl)ester of Carbonic Acid: Spectroscopic Characterization and Improved Preparation
Keywords The low temperature preparation of the bistrimethylsilylester of carbonic acid is reported. The hydrolysable and thermolabile (Me 3 SiO) 2 CO has been characterized by vibrational and NMR spectroscopic methods. Under inert conditions the (Me 3 SiO) 2 CO is stable at 233 K for several weeks.
Published in: | Zeitschrift für Naturforschung B |
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Main Authors: | , |
Format: | Article in Journal/Newspaper |
Language: | English |
Published: |
Walter de Gruyter GmbH
1998
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Subjects: | |
Online Access: | http://dx.doi.org/10.1515/znb-1998-0812 https://www.degruyter.com/view/journals/znb/53/8/article-p849.xml https://www.degruyter.com/document/doi/10.1515/znb-1998-0812/xml https://www.degruyter.com/document/doi/10.1515/znb-1998-0812/pdf |
Summary: | Keywords The low temperature preparation of the bistrimethylsilylester of carbonic acid is reported. The hydrolysable and thermolabile (Me 3 SiO) 2 CO has been characterized by vibrational and NMR spectroscopic methods. Under inert conditions the (Me 3 SiO) 2 CO is stable at 233 K for several weeks. |
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