Qualitative and Quantitative Evaluation of Rosavin, Salidroside, and p-Tyrosol in Artic Root Products via TLC-Screening, HPLC-DAD, and NMR Spectroscopy
Artic root is a well-known plant adaptogen with multipotential pharmacological properties. Thin-layer chromatography (TLC)—screening followed by diode-array high-performance liquid chromatography and nuclear magnetic resonance spectroscopy proved to be a reliable and convenient method for the simult...
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ftpubmed:oai:pubmedcentral.nih.gov:9739797 2023-05-15T15:02:51+02:00 Qualitative and Quantitative Evaluation of Rosavin, Salidroside, and p-Tyrosol in Artic Root Products via TLC-Screening, HPLC-DAD, and NMR Spectroscopy Nikolaichuk, Hanna Studziński, Marek Stankevič, Marek Choma, Irena M. 2022-11-28 http://www.ncbi.nlm.nih.gov/pmc/articles/PMC9739797/ http://www.ncbi.nlm.nih.gov/pubmed/36500392 https://doi.org/10.3390/molecules27238299 en eng MDPI http://www.ncbi.nlm.nih.gov/pmc/articles/PMC9739797/ http://www.ncbi.nlm.nih.gov/pubmed/36500392 http://dx.doi.org/10.3390/molecules27238299 © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). CC-BY Molecules Article Text 2022 ftpubmed https://doi.org/10.3390/molecules27238299 2022-12-18T01:53:51Z Artic root is a well-known plant adaptogen with multipotential pharmacological properties. Thin-layer chromatography (TLC)—screening followed by diode-array high-performance liquid chromatography and nuclear magnetic resonance spectroscopy proved to be a reliable and convenient method for the simultaneous determination of the quality of various herbal raw materials and supplements. This combination allowed for comparing and differentiating arctic root samples as well as defining their authenticity. The study provided information on the chemical and biological properties of the seven chosen samples as well as qualitative and quantitative evaluation of the quality markers: rosavin, salidroside, and p-tyrosol. The absence of rosavin, salidroside, and p-tyrosol in three samples was detected using TLC screening and confirmed by HPLC-DAD and NMR. The paper highlighted the importance of quality control and strict regulation for herbal medicine supplements and preparations. Text Arctic PubMed Central (PMC) Arctic Molecules 27 23 8299 |
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Article Nikolaichuk, Hanna Studziński, Marek Stankevič, Marek Choma, Irena M. Qualitative and Quantitative Evaluation of Rosavin, Salidroside, and p-Tyrosol in Artic Root Products via TLC-Screening, HPLC-DAD, and NMR Spectroscopy |
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Article |
description |
Artic root is a well-known plant adaptogen with multipotential pharmacological properties. Thin-layer chromatography (TLC)—screening followed by diode-array high-performance liquid chromatography and nuclear magnetic resonance spectroscopy proved to be a reliable and convenient method for the simultaneous determination of the quality of various herbal raw materials and supplements. This combination allowed for comparing and differentiating arctic root samples as well as defining their authenticity. The study provided information on the chemical and biological properties of the seven chosen samples as well as qualitative and quantitative evaluation of the quality markers: rosavin, salidroside, and p-tyrosol. The absence of rosavin, salidroside, and p-tyrosol in three samples was detected using TLC screening and confirmed by HPLC-DAD and NMR. The paper highlighted the importance of quality control and strict regulation for herbal medicine supplements and preparations. |
format |
Text |
author |
Nikolaichuk, Hanna Studziński, Marek Stankevič, Marek Choma, Irena M. |
author_facet |
Nikolaichuk, Hanna Studziński, Marek Stankevič, Marek Choma, Irena M. |
author_sort |
Nikolaichuk, Hanna |
title |
Qualitative and Quantitative Evaluation of Rosavin, Salidroside, and p-Tyrosol in Artic Root Products via TLC-Screening, HPLC-DAD, and NMR Spectroscopy |
title_short |
Qualitative and Quantitative Evaluation of Rosavin, Salidroside, and p-Tyrosol in Artic Root Products via TLC-Screening, HPLC-DAD, and NMR Spectroscopy |
title_full |
Qualitative and Quantitative Evaluation of Rosavin, Salidroside, and p-Tyrosol in Artic Root Products via TLC-Screening, HPLC-DAD, and NMR Spectroscopy |
title_fullStr |
Qualitative and Quantitative Evaluation of Rosavin, Salidroside, and p-Tyrosol in Artic Root Products via TLC-Screening, HPLC-DAD, and NMR Spectroscopy |
title_full_unstemmed |
Qualitative and Quantitative Evaluation of Rosavin, Salidroside, and p-Tyrosol in Artic Root Products via TLC-Screening, HPLC-DAD, and NMR Spectroscopy |
title_sort |
qualitative and quantitative evaluation of rosavin, salidroside, and p-tyrosol in artic root products via tlc-screening, hplc-dad, and nmr spectroscopy |
publisher |
MDPI |
publishDate |
2022 |
url |
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC9739797/ http://www.ncbi.nlm.nih.gov/pubmed/36500392 https://doi.org/10.3390/molecules27238299 |
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Arctic |
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Arctic |
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Arctic |
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Arctic |
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Molecules |
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http://www.ncbi.nlm.nih.gov/pmc/articles/PMC9739797/ http://www.ncbi.nlm.nih.gov/pubmed/36500392 http://dx.doi.org/10.3390/molecules27238299 |
op_rights |
© 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
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CC-BY |
op_doi |
https://doi.org/10.3390/molecules27238299 |
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