Nuclear magnetic resonance probe head design for precision strain control
Here, we present the design and construction of an NMR probe to investigate single crystals under strain at cryogenic temperatures. The probe head incorporates a piezoelectric-based apparatus from Razorbill Instruments that enables both compressive and tensile strain tuning up to strain values on th...
Published in: | Review of Scientific Instruments |
---|---|
Main Authors: | , , , , , |
Language: | unknown |
Published: |
2022
|
Subjects: | |
Online Access: | http://www.osti.gov/servlets/purl/1409367 https://www.osti.gov/biblio/1409367 https://doi.org/10.1063/1.5002631 |
id |
ftosti:oai:osti.gov:1409367 |
---|---|
record_format |
openpolar |
spelling |
ftosti:oai:osti.gov:1409367 2023-07-30T04:06:32+02:00 Nuclear magnetic resonance probe head design for precision strain control Kissikov, T. Sarkar, R. Bush, B. T. Lawson, M. Canfield, P. C. Curro, N. J. 2022-05-23 application/pdf http://www.osti.gov/servlets/purl/1409367 https://www.osti.gov/biblio/1409367 https://doi.org/10.1063/1.5002631 unknown http://www.osti.gov/servlets/purl/1409367 https://www.osti.gov/biblio/1409367 https://doi.org/10.1063/1.5002631 doi:10.1063/1.5002631 37 INORGANIC ORGANIC PHYSICAL AND ANALYTICAL CHEMISTRY 2022 ftosti https://doi.org/10.1063/1.5002631 2023-07-11T09:22:56Z Here, we present the design and construction of an NMR probe to investigate single crystals under strain at cryogenic temperatures. The probe head incorporates a piezoelectric-based apparatus from Razorbill Instruments that enables both compressive and tensile strain tuning up to strain values on the order of 0.3% with a precision of 0.001%. 75 As NMR in BaFe 2 As 2 reveals large changes to the electric field gradient and indicates that the strain is homogeneous to within 16% over the volume of the NMR coil. Other/Unknown Material Razorbill SciTec Connect (Office of Scientific and Technical Information - OSTI, U.S. Department of Energy) Review of Scientific Instruments 88 10 103902 |
institution |
Open Polar |
collection |
SciTec Connect (Office of Scientific and Technical Information - OSTI, U.S. Department of Energy) |
op_collection_id |
ftosti |
language |
unknown |
topic |
37 INORGANIC ORGANIC PHYSICAL AND ANALYTICAL CHEMISTRY |
spellingShingle |
37 INORGANIC ORGANIC PHYSICAL AND ANALYTICAL CHEMISTRY Kissikov, T. Sarkar, R. Bush, B. T. Lawson, M. Canfield, P. C. Curro, N. J. Nuclear magnetic resonance probe head design for precision strain control |
topic_facet |
37 INORGANIC ORGANIC PHYSICAL AND ANALYTICAL CHEMISTRY |
description |
Here, we present the design and construction of an NMR probe to investigate single crystals under strain at cryogenic temperatures. The probe head incorporates a piezoelectric-based apparatus from Razorbill Instruments that enables both compressive and tensile strain tuning up to strain values on the order of 0.3% with a precision of 0.001%. 75 As NMR in BaFe 2 As 2 reveals large changes to the electric field gradient and indicates that the strain is homogeneous to within 16% over the volume of the NMR coil. |
author |
Kissikov, T. Sarkar, R. Bush, B. T. Lawson, M. Canfield, P. C. Curro, N. J. |
author_facet |
Kissikov, T. Sarkar, R. Bush, B. T. Lawson, M. Canfield, P. C. Curro, N. J. |
author_sort |
Kissikov, T. |
title |
Nuclear magnetic resonance probe head design for precision strain control |
title_short |
Nuclear magnetic resonance probe head design for precision strain control |
title_full |
Nuclear magnetic resonance probe head design for precision strain control |
title_fullStr |
Nuclear magnetic resonance probe head design for precision strain control |
title_full_unstemmed |
Nuclear magnetic resonance probe head design for precision strain control |
title_sort |
nuclear magnetic resonance probe head design for precision strain control |
publishDate |
2022 |
url |
http://www.osti.gov/servlets/purl/1409367 https://www.osti.gov/biblio/1409367 https://doi.org/10.1063/1.5002631 |
genre |
Razorbill |
genre_facet |
Razorbill |
op_relation |
http://www.osti.gov/servlets/purl/1409367 https://www.osti.gov/biblio/1409367 https://doi.org/10.1063/1.5002631 doi:10.1063/1.5002631 |
op_doi |
https://doi.org/10.1063/1.5002631 |
container_title |
Review of Scientific Instruments |
container_volume |
88 |
container_issue |
10 |
container_start_page |
103902 |
_version_ |
1772819191073603584 |