Dracocephalum palmatum S. and Dracocephalum ruyschiana L. Originating from Yakutia: A High-Resolution Mass Spectrometric Approach for the Comprehensive Characterization of Phenolic Compounds
Dracocephalum palmatum S. and Dracocephalum ruyschiana L. contain a large number of target analytes, which are biologically active compounds. High performance liquid chromatography (HPLC) in combination with an ion trap (tandem mass spectrometry) was used to identify target analytes in extracts of D...
Published in: | Applied Sciences |
---|---|
Main Authors: | , , , , , , , |
Format: | Text |
Language: | English |
Published: |
Multidisciplinary Digital Publishing Institute
2022
|
Subjects: | |
Online Access: | https://doi.org/10.3390/app12031766 |
id |
ftmdpi:oai:mdpi.com:/2076-3417/12/3/1766/ |
---|---|
record_format |
openpolar |
spelling |
ftmdpi:oai:mdpi.com:/2076-3417/12/3/1766/ 2023-08-20T04:10:20+02:00 Dracocephalum palmatum S. and Dracocephalum ruyschiana L. Originating from Yakutia: A High-Resolution Mass Spectrometric Approach for the Comprehensive Characterization of Phenolic Compounds Zhanna M. Okhlopkova Mayya P. Razgonova Konstantin S. Pikula Alexander M. Zakharenko Wojciech Piekoszewski Yuri A. Manakov Sezai Ercisli Kirill S. Golokhvast agris 2022-02-08 application/pdf https://doi.org/10.3390/app12031766 EN eng Multidisciplinary Digital Publishing Institute Applied Biosciences and Bioengineering https://dx.doi.org/10.3390/app12031766 https://creativecommons.org/licenses/by/4.0/ Applied Sciences; Volume 12; Issue 3; Pages: 1766 Dracocephalum palmatum Dracocephalum ruyschiana ion trap tandem mass spectrometry polyphenolic compounds Text 2022 ftmdpi https://doi.org/10.3390/app12031766 2023-08-01T04:06:03Z Dracocephalum palmatum S. and Dracocephalum ruyschiana L. contain a large number of target analytes, which are biologically active compounds. High performance liquid chromatography (HPLC) in combination with an ion trap (tandem mass spectrometry) was used to identify target analytes in extracts of D. palmatum S. and D. ruyschiana L. originating from Yakutia. The results of initial studies revealed the presence of 114 compounds, of which 92 were identified for the first time in the genus Dracocephalum. New identified metabolites belonged to 17 classes, including 16 phenolic acids and their conjugates, 18 flavones, 5 flavonols, 2 flavan-3-ols, 1 flavanone, 2 stilbenes, 10 anthocyanins, 1 condensed tannin, 2 lignans, 6 carotenoids, 3 oxylipins, 2 amino acids, 3 sceletium alkaloids, 3 carboxylic acids, 8 fatty acids, 1 sterol, and 3 terpenes, along with 6 miscellaneous compounds. It was shown that extracts of D. palmatum are richer in the spectrum of polyphenolic compounds compared with extracts of D. ruyschiana, according to a study of the presence of these compounds in extracts, based on the results of mass spectrometric studies. Text Yakutia MDPI Open Access Publishing Applied Sciences 12 3 1766 |
institution |
Open Polar |
collection |
MDPI Open Access Publishing |
op_collection_id |
ftmdpi |
language |
English |
topic |
Dracocephalum palmatum Dracocephalum ruyschiana ion trap tandem mass spectrometry polyphenolic compounds |
spellingShingle |
Dracocephalum palmatum Dracocephalum ruyschiana ion trap tandem mass spectrometry polyphenolic compounds Zhanna M. Okhlopkova Mayya P. Razgonova Konstantin S. Pikula Alexander M. Zakharenko Wojciech Piekoszewski Yuri A. Manakov Sezai Ercisli Kirill S. Golokhvast Dracocephalum palmatum S. and Dracocephalum ruyschiana L. Originating from Yakutia: A High-Resolution Mass Spectrometric Approach for the Comprehensive Characterization of Phenolic Compounds |
topic_facet |
Dracocephalum palmatum Dracocephalum ruyschiana ion trap tandem mass spectrometry polyphenolic compounds |
description |
Dracocephalum palmatum S. and Dracocephalum ruyschiana L. contain a large number of target analytes, which are biologically active compounds. High performance liquid chromatography (HPLC) in combination with an ion trap (tandem mass spectrometry) was used to identify target analytes in extracts of D. palmatum S. and D. ruyschiana L. originating from Yakutia. The results of initial studies revealed the presence of 114 compounds, of which 92 were identified for the first time in the genus Dracocephalum. New identified metabolites belonged to 17 classes, including 16 phenolic acids and their conjugates, 18 flavones, 5 flavonols, 2 flavan-3-ols, 1 flavanone, 2 stilbenes, 10 anthocyanins, 1 condensed tannin, 2 lignans, 6 carotenoids, 3 oxylipins, 2 amino acids, 3 sceletium alkaloids, 3 carboxylic acids, 8 fatty acids, 1 sterol, and 3 terpenes, along with 6 miscellaneous compounds. It was shown that extracts of D. palmatum are richer in the spectrum of polyphenolic compounds compared with extracts of D. ruyschiana, according to a study of the presence of these compounds in extracts, based on the results of mass spectrometric studies. |
format |
Text |
author |
Zhanna M. Okhlopkova Mayya P. Razgonova Konstantin S. Pikula Alexander M. Zakharenko Wojciech Piekoszewski Yuri A. Manakov Sezai Ercisli Kirill S. Golokhvast |
author_facet |
Zhanna M. Okhlopkova Mayya P. Razgonova Konstantin S. Pikula Alexander M. Zakharenko Wojciech Piekoszewski Yuri A. Manakov Sezai Ercisli Kirill S. Golokhvast |
author_sort |
Zhanna M. Okhlopkova |
title |
Dracocephalum palmatum S. and Dracocephalum ruyschiana L. Originating from Yakutia: A High-Resolution Mass Spectrometric Approach for the Comprehensive Characterization of Phenolic Compounds |
title_short |
Dracocephalum palmatum S. and Dracocephalum ruyschiana L. Originating from Yakutia: A High-Resolution Mass Spectrometric Approach for the Comprehensive Characterization of Phenolic Compounds |
title_full |
Dracocephalum palmatum S. and Dracocephalum ruyschiana L. Originating from Yakutia: A High-Resolution Mass Spectrometric Approach for the Comprehensive Characterization of Phenolic Compounds |
title_fullStr |
Dracocephalum palmatum S. and Dracocephalum ruyschiana L. Originating from Yakutia: A High-Resolution Mass Spectrometric Approach for the Comprehensive Characterization of Phenolic Compounds |
title_full_unstemmed |
Dracocephalum palmatum S. and Dracocephalum ruyschiana L. Originating from Yakutia: A High-Resolution Mass Spectrometric Approach for the Comprehensive Characterization of Phenolic Compounds |
title_sort |
dracocephalum palmatum s. and dracocephalum ruyschiana l. originating from yakutia: a high-resolution mass spectrometric approach for the comprehensive characterization of phenolic compounds |
publisher |
Multidisciplinary Digital Publishing Institute |
publishDate |
2022 |
url |
https://doi.org/10.3390/app12031766 |
op_coverage |
agris |
genre |
Yakutia |
genre_facet |
Yakutia |
op_source |
Applied Sciences; Volume 12; Issue 3; Pages: 1766 |
op_relation |
Applied Biosciences and Bioengineering https://dx.doi.org/10.3390/app12031766 |
op_rights |
https://creativecommons.org/licenses/by/4.0/ |
op_doi |
https://doi.org/10.3390/app12031766 |
container_title |
Applied Sciences |
container_volume |
12 |
container_issue |
3 |
container_start_page |
1766 |
_version_ |
1774724453173821440 |