Qualitative and Quantitative Evaluation of Rosavin, Salidroside, and p-Tyrosol in Artic Root Products via TLC-Screening, HPLC-DAD, and NMR Spectroscopy
Artic root is a well-known plant adaptogen with multipotential pharmacological properties. Thin-layer chromatography (TLC)—screening followed by diode-array high-performance liquid chromatography and nuclear magnetic resonance spectroscopy proved to be a reliable and convenient method for the simult...
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MDPI AG
2022
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ftdoajarticles:oai:doaj.org/article:dda89217d33545a6a7b834c507dc21ca 2023-05-15T14:55:15+02:00 Qualitative and Quantitative Evaluation of Rosavin, Salidroside, and p-Tyrosol in Artic Root Products via TLC-Screening, HPLC-DAD, and NMR Spectroscopy Hanna Nikolaichuk Marek Studziński Marek Stankevič Irena M. Choma 2022-11-01T00:00:00Z https://doi.org/10.3390/molecules27238299 https://doaj.org/article/dda89217d33545a6a7b834c507dc21ca EN eng MDPI AG https://www.mdpi.com/1420-3049/27/23/8299 https://doaj.org/toc/1420-3049 doi:10.3390/molecules27238299 1420-3049 https://doaj.org/article/dda89217d33545a6a7b834c507dc21ca Molecules, Vol 27, Iss 8299, p 8299 (2022) TLC-screening HPLC-DAD NMR arctic root Organic chemistry QD241-441 article 2022 ftdoajarticles https://doi.org/10.3390/molecules27238299 2022-12-30T19:35:58Z Artic root is a well-known plant adaptogen with multipotential pharmacological properties. Thin-layer chromatography (TLC)—screening followed by diode-array high-performance liquid chromatography and nuclear magnetic resonance spectroscopy proved to be a reliable and convenient method for the simultaneous determination of the quality of various herbal raw materials and supplements. This combination allowed for comparing and differentiating arctic root samples as well as defining their authenticity. The study provided information on the chemical and biological properties of the seven chosen samples as well as qualitative and quantitative evaluation of the quality markers: rosavin, salidroside, and p-tyrosol. The absence of rosavin, salidroside, and p-tyrosol in three samples was detected using TLC screening and confirmed by HPLC-DAD and NMR. The paper highlighted the importance of quality control and strict regulation for herbal medicine supplements and preparations. Article in Journal/Newspaper Arctic Directory of Open Access Journals: DOAJ Articles Arctic Molecules 27 23 8299 |
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Open Polar |
collection |
Directory of Open Access Journals: DOAJ Articles |
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ftdoajarticles |
language |
English |
topic |
TLC-screening HPLC-DAD NMR arctic root Organic chemistry QD241-441 |
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TLC-screening HPLC-DAD NMR arctic root Organic chemistry QD241-441 Hanna Nikolaichuk Marek Studziński Marek Stankevič Irena M. Choma Qualitative and Quantitative Evaluation of Rosavin, Salidroside, and p-Tyrosol in Artic Root Products via TLC-Screening, HPLC-DAD, and NMR Spectroscopy |
topic_facet |
TLC-screening HPLC-DAD NMR arctic root Organic chemistry QD241-441 |
description |
Artic root is a well-known plant adaptogen with multipotential pharmacological properties. Thin-layer chromatography (TLC)—screening followed by diode-array high-performance liquid chromatography and nuclear magnetic resonance spectroscopy proved to be a reliable and convenient method for the simultaneous determination of the quality of various herbal raw materials and supplements. This combination allowed for comparing and differentiating arctic root samples as well as defining their authenticity. The study provided information on the chemical and biological properties of the seven chosen samples as well as qualitative and quantitative evaluation of the quality markers: rosavin, salidroside, and p-tyrosol. The absence of rosavin, salidroside, and p-tyrosol in three samples was detected using TLC screening and confirmed by HPLC-DAD and NMR. The paper highlighted the importance of quality control and strict regulation for herbal medicine supplements and preparations. |
format |
Article in Journal/Newspaper |
author |
Hanna Nikolaichuk Marek Studziński Marek Stankevič Irena M. Choma |
author_facet |
Hanna Nikolaichuk Marek Studziński Marek Stankevič Irena M. Choma |
author_sort |
Hanna Nikolaichuk |
title |
Qualitative and Quantitative Evaluation of Rosavin, Salidroside, and p-Tyrosol in Artic Root Products via TLC-Screening, HPLC-DAD, and NMR Spectroscopy |
title_short |
Qualitative and Quantitative Evaluation of Rosavin, Salidroside, and p-Tyrosol in Artic Root Products via TLC-Screening, HPLC-DAD, and NMR Spectroscopy |
title_full |
Qualitative and Quantitative Evaluation of Rosavin, Salidroside, and p-Tyrosol in Artic Root Products via TLC-Screening, HPLC-DAD, and NMR Spectroscopy |
title_fullStr |
Qualitative and Quantitative Evaluation of Rosavin, Salidroside, and p-Tyrosol in Artic Root Products via TLC-Screening, HPLC-DAD, and NMR Spectroscopy |
title_full_unstemmed |
Qualitative and Quantitative Evaluation of Rosavin, Salidroside, and p-Tyrosol in Artic Root Products via TLC-Screening, HPLC-DAD, and NMR Spectroscopy |
title_sort |
qualitative and quantitative evaluation of rosavin, salidroside, and p-tyrosol in artic root products via tlc-screening, hplc-dad, and nmr spectroscopy |
publisher |
MDPI AG |
publishDate |
2022 |
url |
https://doi.org/10.3390/molecules27238299 https://doaj.org/article/dda89217d33545a6a7b834c507dc21ca |
geographic |
Arctic |
geographic_facet |
Arctic |
genre |
Arctic |
genre_facet |
Arctic |
op_source |
Molecules, Vol 27, Iss 8299, p 8299 (2022) |
op_relation |
https://www.mdpi.com/1420-3049/27/23/8299 https://doaj.org/toc/1420-3049 doi:10.3390/molecules27238299 1420-3049 https://doaj.org/article/dda89217d33545a6a7b834c507dc21ca |
op_doi |
https://doi.org/10.3390/molecules27238299 |
container_title |
Molecules |
container_volume |
27 |
container_issue |
23 |
container_start_page |
8299 |
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1766327037411196928 |