Lipase-Catalyzed Solvent-Free Amidation of Phenolic Acids
A series of N-alkyl-substituted amides, based on various phenolic acids, have been synthesized by the condensation of equimolar amounts of phenolic acids with different alkyl amines in the presence of Candida antarctica lipase at 60–90 °C in 16–20 h. The reactions were carried out in a solvent-free...
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ftdatacite:10.6084/m9.figshare.1226505.v3 2023-05-15T13:44:05+02:00 Lipase-Catalyzed Solvent-Free Amidation of Phenolic Acids Parshant Kaushik Najam Akhtar Shakil Jitendra Kumar Braj Bhushan Singh 2015 https://dx.doi.org/10.6084/m9.figshare.1226505.v3 https://tandf.figshare.com/articles/journal_contribution/Lipase_Catalyzed_Solvent_Free_Amidation_of_Phenolic_Acids/1226505/3 unknown Taylor & Francis https://dx.doi.org/10.1080/00397911.2014.974611 https://dx.doi.org/10.6084/m9.figshare.1226505 Creative Commons Attribution 4.0 International https://creativecommons.org/licenses/by/4.0/legalcode cc-by-4.0 CC-BY Sociology FOS Sociology Biotechnology Biological Sciences Chemistry Earth and Environmental Sciences Biochemistry Text article-journal Journal contribution ScholarlyArticle 2015 ftdatacite https://doi.org/10.6084/m9.figshare.1226505.v3 https://doi.org/10.1080/00397911.2014.974611 https://doi.org/10.6084/m9.figshare.1226505 2021-11-05T12:55:41Z A series of N-alkyl-substituted amides, based on various phenolic acids, have been synthesized by the condensation of equimolar amounts of phenolic acids with different alkyl amines in the presence of Candida antarctica lipase at 60–90 °C in 16–20 h. The reactions were carried out in a solvent-free system without the use of any activating agents. All the products were obtained in appreciable amounts and the yields for different compounds varied between 75.6% and 83.5%. The synthesized compounds were characterized using spectroscopy techniques, namely infrared and NMR ( 1 H and 13 C). Text Antarc* Antarctica DataCite Metadata Store (German National Library of Science and Technology) |
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Sociology FOS Sociology Biotechnology Biological Sciences Chemistry Earth and Environmental Sciences Biochemistry |
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Sociology FOS Sociology Biotechnology Biological Sciences Chemistry Earth and Environmental Sciences Biochemistry Parshant Kaushik Najam Akhtar Shakil Jitendra Kumar Braj Bhushan Singh Lipase-Catalyzed Solvent-Free Amidation of Phenolic Acids |
topic_facet |
Sociology FOS Sociology Biotechnology Biological Sciences Chemistry Earth and Environmental Sciences Biochemistry |
description |
A series of N-alkyl-substituted amides, based on various phenolic acids, have been synthesized by the condensation of equimolar amounts of phenolic acids with different alkyl amines in the presence of Candida antarctica lipase at 60–90 °C in 16–20 h. The reactions were carried out in a solvent-free system without the use of any activating agents. All the products were obtained in appreciable amounts and the yields for different compounds varied between 75.6% and 83.5%. The synthesized compounds were characterized using spectroscopy techniques, namely infrared and NMR ( 1 H and 13 C). |
format |
Text |
author |
Parshant Kaushik Najam Akhtar Shakil Jitendra Kumar Braj Bhushan Singh |
author_facet |
Parshant Kaushik Najam Akhtar Shakil Jitendra Kumar Braj Bhushan Singh |
author_sort |
Parshant Kaushik |
title |
Lipase-Catalyzed Solvent-Free Amidation of Phenolic Acids |
title_short |
Lipase-Catalyzed Solvent-Free Amidation of Phenolic Acids |
title_full |
Lipase-Catalyzed Solvent-Free Amidation of Phenolic Acids |
title_fullStr |
Lipase-Catalyzed Solvent-Free Amidation of Phenolic Acids |
title_full_unstemmed |
Lipase-Catalyzed Solvent-Free Amidation of Phenolic Acids |
title_sort |
lipase-catalyzed solvent-free amidation of phenolic acids |
publisher |
Taylor & Francis |
publishDate |
2015 |
url |
https://dx.doi.org/10.6084/m9.figshare.1226505.v3 https://tandf.figshare.com/articles/journal_contribution/Lipase_Catalyzed_Solvent_Free_Amidation_of_Phenolic_Acids/1226505/3 |
genre |
Antarc* Antarctica |
genre_facet |
Antarc* Antarctica |
op_relation |
https://dx.doi.org/10.1080/00397911.2014.974611 https://dx.doi.org/10.6084/m9.figshare.1226505 |
op_rights |
Creative Commons Attribution 4.0 International https://creativecommons.org/licenses/by/4.0/legalcode cc-by-4.0 |
op_rightsnorm |
CC-BY |
op_doi |
https://doi.org/10.6084/m9.figshare.1226505.v3 https://doi.org/10.1080/00397911.2014.974611 https://doi.org/10.6084/m9.figshare.1226505 |
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1766197693220126720 |