Data on the spatial distribution of 1,1-dimethylhydrazine and its transformation products in peat bog soil of rocket stage fall place in Russian North
The data set covers the results of a study of 96 samples of peat bog soil from the fall place of the first stage of the Cyclone-3 launch vehicle (launched from Plesetsk Cosmodrome in 2004) contained unburned toxic rocket fuel 1,1-dimethylhydrazine (UDMH) in the European North of Russia. The fall pla...
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ftdatacite:10.17632/xxrfygp99g 2023-05-15T18:08:00+02:00 Data on the spatial distribution of 1,1-dimethylhydrazine and its transformation products in peat bog soil of rocket stage fall place in Russian North Kosyakov, Dmitry 2020 https://dx.doi.org/10.17632/xxrfygp99g https://data.mendeley.com/datasets/xxrfygp99g unknown Mendeley https://dx.doi.org/10.17632/xxrfygp99g.1 Creative Commons Attribution 4.0 International info:eu-repo/semantics/openAccess https://creativecommons.org/licenses/by/4.0/legalcode cc-by-4.0 CC-BY Analytical Chemistry FOS Chemical sciences Chemical Ecology Soil Environmental Assessment Rocket Peat Bog dataset Dataset 2020 ftdatacite https://doi.org/10.17632/xxrfygp99g https://doi.org/10.17632/xxrfygp99g.1 2021-11-05T12:55:41Z The data set covers the results of a study of 96 samples of peat bog soil from the fall place of the first stage of the Cyclone-3 launch vehicle (launched from Plesetsk Cosmodrome in 2004) contained unburned toxic rocket fuel 1,1-dimethylhydrazine (UDMH) in the European North of Russia. The fall place is located in a peat bog and contains a round central crater (diameter of 6 m) filled with swamp water. There are two data files in this data set. Data file 1 (Excel spreadsheet) presents the concentrations of hydrazines (UDMH; methylhydrazine, MT; and hydrazine, H) in soil samples determined by hydrophilic interaction liquid chromatography with amperometric detection after steam distillation of analytes from alkaline medium. Data file 2 (Excel spreadsheet) presents the concentrations of eight UDMH transformation products (1,1,4,4-tetramethyltetrazene, TMT; formaldehyde N,N-dimethylhydrazone, DMHF; acetaldehyde N,N-dimethylhydrazone, DMHA; furaldehyde N,N-dimethylhydrazone, DMHFur; 1-formyl-2,2-dimethylhydrazine, FADMH; N,N-dimethylformamide, DMF; N-nitrosodimethylamine, NDMA; and 1-methyl-1H-1,2,4-triazole, MT) determined by gas chromatography – tandem mass spectrometry after pressurized liquid extraction of soil samples. The concentration values in both data files were calculated for initial wet soil samples and oven-dried ones using the data on moisture content also presented in the Excel spreadsheets. All concentrations are presented with standard deviation value calculated on the basis of three replicate analyses of each soil sample. Sampling point designations are given in the following format: Cardinal direction (N, S, W, E) – distance from the central crater (m). Dataset Russian North DataCite Metadata Store (German National Library of Science and Technology) Plesetsk ENVELOPE(40.292,40.292,62.708,62.708) |
institution |
Open Polar |
collection |
DataCite Metadata Store (German National Library of Science and Technology) |
op_collection_id |
ftdatacite |
language |
unknown |
topic |
Analytical Chemistry FOS Chemical sciences Chemical Ecology Soil Environmental Assessment Rocket Peat Bog |
spellingShingle |
Analytical Chemistry FOS Chemical sciences Chemical Ecology Soil Environmental Assessment Rocket Peat Bog Kosyakov, Dmitry Data on the spatial distribution of 1,1-dimethylhydrazine and its transformation products in peat bog soil of rocket stage fall place in Russian North |
topic_facet |
Analytical Chemistry FOS Chemical sciences Chemical Ecology Soil Environmental Assessment Rocket Peat Bog |
description |
The data set covers the results of a study of 96 samples of peat bog soil from the fall place of the first stage of the Cyclone-3 launch vehicle (launched from Plesetsk Cosmodrome in 2004) contained unburned toxic rocket fuel 1,1-dimethylhydrazine (UDMH) in the European North of Russia. The fall place is located in a peat bog and contains a round central crater (diameter of 6 m) filled with swamp water. There are two data files in this data set. Data file 1 (Excel spreadsheet) presents the concentrations of hydrazines (UDMH; methylhydrazine, MT; and hydrazine, H) in soil samples determined by hydrophilic interaction liquid chromatography with amperometric detection after steam distillation of analytes from alkaline medium. Data file 2 (Excel spreadsheet) presents the concentrations of eight UDMH transformation products (1,1,4,4-tetramethyltetrazene, TMT; formaldehyde N,N-dimethylhydrazone, DMHF; acetaldehyde N,N-dimethylhydrazone, DMHA; furaldehyde N,N-dimethylhydrazone, DMHFur; 1-formyl-2,2-dimethylhydrazine, FADMH; N,N-dimethylformamide, DMF; N-nitrosodimethylamine, NDMA; and 1-methyl-1H-1,2,4-triazole, MT) determined by gas chromatography – tandem mass spectrometry after pressurized liquid extraction of soil samples. The concentration values in both data files were calculated for initial wet soil samples and oven-dried ones using the data on moisture content also presented in the Excel spreadsheets. All concentrations are presented with standard deviation value calculated on the basis of three replicate analyses of each soil sample. Sampling point designations are given in the following format: Cardinal direction (N, S, W, E) – distance from the central crater (m). |
format |
Dataset |
author |
Kosyakov, Dmitry |
author_facet |
Kosyakov, Dmitry |
author_sort |
Kosyakov, Dmitry |
title |
Data on the spatial distribution of 1,1-dimethylhydrazine and its transformation products in peat bog soil of rocket stage fall place in Russian North |
title_short |
Data on the spatial distribution of 1,1-dimethylhydrazine and its transformation products in peat bog soil of rocket stage fall place in Russian North |
title_full |
Data on the spatial distribution of 1,1-dimethylhydrazine and its transformation products in peat bog soil of rocket stage fall place in Russian North |
title_fullStr |
Data on the spatial distribution of 1,1-dimethylhydrazine and its transformation products in peat bog soil of rocket stage fall place in Russian North |
title_full_unstemmed |
Data on the spatial distribution of 1,1-dimethylhydrazine and its transformation products in peat bog soil of rocket stage fall place in Russian North |
title_sort |
data on the spatial distribution of 1,1-dimethylhydrazine and its transformation products in peat bog soil of rocket stage fall place in russian north |
publisher |
Mendeley |
publishDate |
2020 |
url |
https://dx.doi.org/10.17632/xxrfygp99g https://data.mendeley.com/datasets/xxrfygp99g |
long_lat |
ENVELOPE(40.292,40.292,62.708,62.708) |
geographic |
Plesetsk |
geographic_facet |
Plesetsk |
genre |
Russian North |
genre_facet |
Russian North |
op_relation |
https://dx.doi.org/10.17632/xxrfygp99g.1 |
op_rights |
Creative Commons Attribution 4.0 International info:eu-repo/semantics/openAccess https://creativecommons.org/licenses/by/4.0/legalcode cc-by-4.0 |
op_rightsnorm |
CC-BY |
op_doi |
https://doi.org/10.17632/xxrfygp99g https://doi.org/10.17632/xxrfygp99g.1 |
_version_ |
1766180234755833856 |