Development of a 450 nm Laser Irradiation Desorption Method for Fast Headspace Solid‐Phase Microextraction of Volatiles from Krill Oil ( Euphausia superba)
A laser irradiation desorption (LID) method is developed using a 450 nm blue semiconductor laser and gas chromatography mass spectrometry (GC/MS) for analyzing the flavor of Antarctic krill oil ( Euphausia superba ). The experimental parameters of LID are optimized by response surface methodology (R...
Published in: | European Journal of Lipid Science and Technology |
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Online Access: | http://dx.doi.org/10.1002/ejlt.201800446 https://api.wiley.com/onlinelibrary/tdm/v1/articles/10.1002%2Fejlt.201800446 https://onlinelibrary.wiley.com/doi/pdf/10.1002/ejlt.201800446 https://onlinelibrary.wiley.com/doi/full-xml/10.1002/ejlt.201800446 |
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crwiley:10.1002/ejlt.201800446 2024-06-23T07:45:51+00:00 Development of a 450 nm Laser Irradiation Desorption Method for Fast Headspace Solid‐Phase Microextraction of Volatiles from Krill Oil ( Euphausia superba) Song, Gongshuai Zhang, Mengna Zhang, Yanping Wang, Honghai Chen, Kang Dai, Zhiyuan Shen, Qing Public Welfare Research Program of Zhejiang Province Zhejiang Provincial R&D Program Natural Science Fund for Young Scholars of China Young Scholars of China 2019 http://dx.doi.org/10.1002/ejlt.201800446 https://api.wiley.com/onlinelibrary/tdm/v1/articles/10.1002%2Fejlt.201800446 https://onlinelibrary.wiley.com/doi/pdf/10.1002/ejlt.201800446 https://onlinelibrary.wiley.com/doi/full-xml/10.1002/ejlt.201800446 en eng Wiley http://onlinelibrary.wiley.com/termsAndConditions#vor European Journal of Lipid Science and Technology volume 121, issue 4 ISSN 1438-7697 1438-9312 journal-article 2019 crwiley https://doi.org/10.1002/ejlt.201800446 2024-06-11T04:43:09Z A laser irradiation desorption (LID) method is developed using a 450 nm blue semiconductor laser and gas chromatography mass spectrometry (GC/MS) for analyzing the flavor of Antarctic krill oil ( Euphausia superba ). The experimental parameters of LID are optimized by response surface methodology (RSM), and the optima are obtained as follows; laser power (10 W), irradiation time (5 min), and sample volume (3 g). The results show that a total of 41 volatile molecular species are detected, including six alcohols, 10 aldehydes, five ketones, 14 hydrocarbons, and six other compounds. Compared with the conventional heating assisted desorption technique, the LID can release volatile molecular species with higher abundance in a considerably reduced extraction time from 30 to 5 min. Finally, the proposed method is validated in terms of sensitivity, precision, linearity, and recovery, which demonstrate its advantages of high efficiency and simplified procedure. Practical Applications : An LID method is developed using a 450 nm blue semiconductor laser for analyzing the flavor of Antarctic krill oil ( E. superba ). Compared with the conventional heating assisted desorption technique, the LID can release more volatile molecular species with higher abundance in a considerably shorter extraction time, and the intensive laser power does not induce the autoxidation of polyunsaturated fatty acids. It shows the advantages of a highly efficient, and simplified procedure. A laser irradiation desorption (LID) method is developed using a 450 nm blue semiconductor laser for analyzing the flavor of Antarctic krill oil ( Euphausia superba ). Article in Journal/Newspaper Antarc* Antarctic Antarctic Krill Euphausia superba Wiley Online Library Antarctic European Journal of Lipid Science and Technology 121 4 1800446 |
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Open Polar |
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Wiley Online Library |
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crwiley |
language |
English |
description |
A laser irradiation desorption (LID) method is developed using a 450 nm blue semiconductor laser and gas chromatography mass spectrometry (GC/MS) for analyzing the flavor of Antarctic krill oil ( Euphausia superba ). The experimental parameters of LID are optimized by response surface methodology (RSM), and the optima are obtained as follows; laser power (10 W), irradiation time (5 min), and sample volume (3 g). The results show that a total of 41 volatile molecular species are detected, including six alcohols, 10 aldehydes, five ketones, 14 hydrocarbons, and six other compounds. Compared with the conventional heating assisted desorption technique, the LID can release volatile molecular species with higher abundance in a considerably reduced extraction time from 30 to 5 min. Finally, the proposed method is validated in terms of sensitivity, precision, linearity, and recovery, which demonstrate its advantages of high efficiency and simplified procedure. Practical Applications : An LID method is developed using a 450 nm blue semiconductor laser for analyzing the flavor of Antarctic krill oil ( E. superba ). Compared with the conventional heating assisted desorption technique, the LID can release more volatile molecular species with higher abundance in a considerably shorter extraction time, and the intensive laser power does not induce the autoxidation of polyunsaturated fatty acids. It shows the advantages of a highly efficient, and simplified procedure. A laser irradiation desorption (LID) method is developed using a 450 nm blue semiconductor laser for analyzing the flavor of Antarctic krill oil ( Euphausia superba ). |
author2 |
Public Welfare Research Program of Zhejiang Province Zhejiang Provincial R&D Program Natural Science Fund for Young Scholars of China Young Scholars of China |
format |
Article in Journal/Newspaper |
author |
Song, Gongshuai Zhang, Mengna Zhang, Yanping Wang, Honghai Chen, Kang Dai, Zhiyuan Shen, Qing |
spellingShingle |
Song, Gongshuai Zhang, Mengna Zhang, Yanping Wang, Honghai Chen, Kang Dai, Zhiyuan Shen, Qing Development of a 450 nm Laser Irradiation Desorption Method for Fast Headspace Solid‐Phase Microextraction of Volatiles from Krill Oil ( Euphausia superba) |
author_facet |
Song, Gongshuai Zhang, Mengna Zhang, Yanping Wang, Honghai Chen, Kang Dai, Zhiyuan Shen, Qing |
author_sort |
Song, Gongshuai |
title |
Development of a 450 nm Laser Irradiation Desorption Method for Fast Headspace Solid‐Phase Microextraction of Volatiles from Krill Oil ( Euphausia superba) |
title_short |
Development of a 450 nm Laser Irradiation Desorption Method for Fast Headspace Solid‐Phase Microextraction of Volatiles from Krill Oil ( Euphausia superba) |
title_full |
Development of a 450 nm Laser Irradiation Desorption Method for Fast Headspace Solid‐Phase Microextraction of Volatiles from Krill Oil ( Euphausia superba) |
title_fullStr |
Development of a 450 nm Laser Irradiation Desorption Method for Fast Headspace Solid‐Phase Microextraction of Volatiles from Krill Oil ( Euphausia superba) |
title_full_unstemmed |
Development of a 450 nm Laser Irradiation Desorption Method for Fast Headspace Solid‐Phase Microextraction of Volatiles from Krill Oil ( Euphausia superba) |
title_sort |
development of a 450 nm laser irradiation desorption method for fast headspace solid‐phase microextraction of volatiles from krill oil ( euphausia superba) |
publisher |
Wiley |
publishDate |
2019 |
url |
http://dx.doi.org/10.1002/ejlt.201800446 https://api.wiley.com/onlinelibrary/tdm/v1/articles/10.1002%2Fejlt.201800446 https://onlinelibrary.wiley.com/doi/pdf/10.1002/ejlt.201800446 https://onlinelibrary.wiley.com/doi/full-xml/10.1002/ejlt.201800446 |
geographic |
Antarctic |
geographic_facet |
Antarctic |
genre |
Antarc* Antarctic Antarctic Krill Euphausia superba |
genre_facet |
Antarc* Antarctic Antarctic Krill Euphausia superba |
op_source |
European Journal of Lipid Science and Technology volume 121, issue 4 ISSN 1438-7697 1438-9312 |
op_rights |
http://onlinelibrary.wiley.com/termsAndConditions#vor |
op_doi |
https://doi.org/10.1002/ejlt.201800446 |
container_title |
European Journal of Lipid Science and Technology |
container_volume |
121 |
container_issue |
4 |
container_start_page |
1800446 |
_version_ |
1802642688992870400 |