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antarctic ice aqueous process stream treatment cdcc cim cooled disc column crystallizer coupled heat and mass transfer crystal growth on a cold surface crystallization cyclic innovation model epsomite eutectic freeze crystallization inline conductivity measurement inline refractive index measurement inline supersaturation determination interface irreversible thermodynamics magnesium sulfate meridianiite mgso4.11h2o micro raman spectroscopy mineral negative crystal non-equilibrium thermodynamics onsager relations saroma lake scale-up sea ice skid mounted unit tga thermogravimetric analysis